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on .net using .net crystal todraw barcode with asp . Polymerizations with narrow molecular weight distribution are chieved at temperatures as high as 35 C in methylene chloride. The polymerization rates are low unless a Lewis acid is present together with the aluminum prophyrin. The Lewis acid coordinates with the carbonyl group of the monomer, which results in suppression of the side reactions as well as activation of the carbon carbon double bond to nucleophilic attack by the initiator. The Lewis acid must be sterically hindered to prevent attack by the nucleophilic initiator on the carbonyl group. Thus, aluminum orthosubstituted phenolates such as methylaluminum bis(2,6-di-t-butyl-4-.methylphenolate) accelerate the polymerization by factors up to 103 104 even at room temperature while maintaining the living character of the eaction. Less sterically hindered Lewis acids, including the aluminum phenolates without ortho substituents, result in loss of the living character and even complete lack of polymerization, unless the reaction temperature is lowered to about 40 C. Steric crowding between the porphyrin structure and the Lewis acid is the key to minimizing side reactions and allowing living polymerization to proceed. The aluminum propyrin initiators are discussed further in Sec. 7-2a-1. Polymerizations of vinyl ketones such as methyl vinyl ketone are also complicated by nucleophilic attack of the initiator and propagating carbanion at the carbonyl group although few details have been established [Dotcheva and Tsvetanov, 1985; Hrdlovic et al., 1979; Nasrallah and Baylouzian, 1977]. Nucleophilic attack in these polymers results in addition, while that at the ester carbonyl of acrylates and methacrylates yields substitution. The major side reaction is an intramolecular aldol-type condensation. Abstraction of an a-hydrogen from a methyl group of the polymer by either initiator or propagating carbanion yields an a-carbanion that attacks the carbonyl group of the adjacent repeat unit.Related: java ean 13 reader Java Barcode Reader Tutorial to scan, read linear, 2d barcodes in ...
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